مشخصات پژوهش

صفحه نخست /Rapid analysis of Achillea ...
عنوان
Rapid analysis of Achillea tenuifolia Lam essential oils by polythiophene/hexagonally ordered silica nanocomposite coating as a solid-phase microextraction fibre
عنوان مجله NATURAL PRODUCT RESEARCH
نوع پژوهش مقاله چاپ شده
کلیدواژه‌ها
polythiophene, hexagonally ordered silica nanocomposite, solid-phase microextraction (SPME), essential oil, Achillea tenuifolia, microwave-assisted extraction
چکیده
Abstract In this work, a highly porous fibre coated with polythiophene/hexagonally ordered silica nanocomposite (PT/SBA-15) was prepared and used for extraction of essential oils with microwave-assisted distillation headspace solid phase microextraction (MA-HS-SPME) method. The prepared nanomaterials were immobilised on a stainless steel wire for fabrication of the SPME fibre. Using MA-HS-SPME followed by GC-MS, 24 compounds were separated and identified in Achillea tenuifolia, which mainly included limonene (28.6%), α-cadinol (12.7%), borneol (6.7%), caryophyllene oxide (3.2%), bornyl acetate (4.3%), camphene (3.2%) and para-cymene (2.3%). The experimental results showed that the polythiophene/hexagonally ordered silica nanocomposite fibres were suitable for the semi-quantitative study of the composition of essential oils in plant materials and for monitoring the variations in the volatile components of the plants.
پژوهشگران مرضیهپیریائی (نفر اول)، مهدیابوالقاسمی (نفر دوم)، حسینناظمیه (نفر سوم)