عنوان
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Determination and analysis of volatile components fromThymus kotschyanus Boiss with a new solid‐phase microextraction fibre and microwave‐assisted hydrodistillation by periodic mesoporous organosilica based on alkylimidazolium ionic liquid
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نوع پژوهش
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مقاله چاپشده در مجلات علمی
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کلیدواژهها
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essential oil, gas chromatography–mass spectrometry, microwave‐assisted hydrodistillation, periodic mesoporous organosilica Ionic liquid, solid‐phase microextraction
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چکیده
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Abstract Introduction: Research on the volatile oil composition of Thymus kotschyanus Boiss was conducted by applying mesoporous organosilica based on alkylimidazolium ionic liquid (PMO‐IL) as a fibre coating material via a method referred to as microwaveassisted headspace solid‐phase microextraction (MA‐HS‐SPME). Methodology: This technique entails microwave irradiation of the sample and collection of the volatile sample components. These components are further introduced into a gas chromatography–mass spectrometry (GC–MS) injection port for further analysis. A simplex method was used for the optimisation of three different parameters affecting the efficiency of the extraction. Conclusion: The MA‐HS‐SPME method proved to be the most suitable technique in oil determination and extraction from Thymus kotschyanus owing to its advantageous aspects of cost effectiveness, simplicity and solvent independence.
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پژوهشگران
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مرضیه پیریائی (نفر اول)، مهدی ابوالقاسمی (نفر دوم)، بابک کریمی (نفر سوم)
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